Wednesday 8 April 2020



OBJECTIVE

To introduce the students to the method of making a mechanical grain size analysis of a soil and presenting the resulting data.

THEORY

Grain size analysis carries much importance in determination of engineering properties of soil e.g. suitability criteria of soils (for road, airfield, levee, dam and foundation material), soil water movement, susceptibility to frost action etc.

The grain size analysis is the attempt to determine the relative proportions of the different grain sizes which make up soil mass. For this, sample should be statically representative of the soil mass.

By carrying out mechanical analysis, particle sizes and their relative distribution can be done for the particle greater than 0.075 mm. The mechanical analysis is carried out by stacking the sieves, one on top of the other, pouring a known weight of soil into the top sieve on the stack, and shaking the sieve in a certain manner to allow the soil to fall down through the stack.

The stack of sieves is known as nest of sieves. The nest is arranged with the largest screen openings (smallest sieve number) on top, progressing to the sieve with the smallest screen opening (largest sieve number) on the bottom of the nest. A lid is placed on the top of the nest and pan is placed below the bottom sieve to catch any soil that passes through the smallest opening. The number or the sizes of the sieves used in the nest depends on the type of the soil and the distribution of the particle sizes. Generally sieve No. 4, 10, 40, 100, 200 are used for classifying the soil.

APPARATUS

1.      A set of sieves
2.      Mechanical soil pulverizer
3.      Weighing balance (Least count = 0.01 grams)
4.      Mechanical sieve shaker


PROCEDURE

1.      Obtain 500 grams of soil sample which has already been pulverized by placing it on sieve No. 200 and then oven dried.
2.      Arrange a nest of sieves including sieves No. 4, 10, 40, 50, 100, 200, pan.
3.      Place the set of sieves in the mechanical sieve shaker and sieve it for 5 to 10 minutes. Note that if the entire set of sieves does not fit into the shaker perform a hand shaking operation until the top few sieves can be removed from the stack and then place the remainder of the stack in the mechanical shaker.
4.      Remove the nest of sieves from the shaker and obtained the weight of the material retained on each sieve. Sum these weights and compare with the actual weight taken. A loss of more than 2 percent by the weight of the residual material is considered unsatisfactory and the test should be replaced.
5.      Compute the percent retained on each sieve by dividing the weight retained on each sieve by the original sample weight.
6.      Compute the percent passing by starting with 100 percent and subtracting the cumulative percent retained for that sieve.
OBSERVATIONS AND CALCULATIONS

Weight of sample = __________ grams

Sieve No.
Diameter
(mm)
Weight of Soil Retained (grams)
Percentage
WeightRetained
(%)
Cumulative Percent Retained
(%)
Percent Passing
(%)






































D10 =                                                                D30 =                                                    D60 = 

                                                      Cu = (D60) / (D10)   

                                       Cc = (D30)2 / (D10) x (D60)

PRECAUTIONS

1.      Particles that appear to be stuck in the sieve screen should never be forced on through the mesh. There are two reasons for not doing this.
a)      The particles would have passed the screen on their own had they been smaller than the mesh opening. Forcing these particles through the screen to be retained on the next size would distort the grain size results.
b)      Secondly forcing the particles through the mesh can damage the screen and necessitate its replacement.

Particles caught in a screen should be removed by brushing with the proper sieve brush. Brushing should be done from the underside of the screen in order that the particles can be brushed out of the screen in the direction from which it entered in the screen opening. Stubborn (obstinate) particles that cannot be removed by rushing should be left in place.

2.      Lumps of soils must have broken down into their individual particles in order for the grain size analysis to be valid. This is accomplished in two ways. The first is to break up lumps with a rubber-tipped pestle in ceramic mortar. It has been found that the rubber-tipped pestles will not grind or crush the individual particles while a ceramic or metal-tipped pestle will.The second is to wet-sieve the soil. Washing the particles that are retained on the No.200 sieve with water and this will accomplish two things.
a)      It separates those small lumps that might not have been broken up with the rubber tipped pestle into individual particles.
b)      It washes the “Dust size” particles and through the No.200 sieve.

3.      A 10 minute shaking period is suggested in procedure. A large sample is requires longer shaking than a sample. Similarly a sample comprising primarily of fine grained material will require a longer shaking period than a coarse grained sample of equal weight.

REFERENCE:
ASTM D422
Standard Test Method for Particle-Size Analysis of Soils

COMMENTS:

Sunday 27 October 2019


OBJECTIVE:

To familiarize the students with general method of obtaining the specific gravity of a mass of any type of material composed of small particles (specifically soil).

THEORY

A value of specific gravity is necessary to compute the void ratio of a soil, it is used in the hydrometer analysis, and it is useful to predict the unit weight of a soil. Occasionally, the specific gravity may be useful in soil mineral classification; e.g., iron minerals have larger value of specific gravity than silicas.

The specific gravity of any substance is defined as the unit weight of the material divided by the unit weight of distilled water at 4 oC. Thu, specific gravity of soil can be found as;
  
As long as equal volume of water and soil are involved, the above stated form can be simplified as;
  

Strictly speaking above mentioned equation is only valid if we do not consider any density change with temperature. However, a slight increase in precision to account for temperature effects on the density of water can be obtained by rewriting above stated equation as;
Where, α is the ratio of the unit weight of water at temperature T of the test and at 4oC. The value of Gs obtained at temperature T (which will be too large if T > 4oC) is appropriately reduced.


APPARATUS

1.      Pycnometer
2.      Weighing balance (Least count of 0.01 grams)
3.      Thermometer
4.      Hot plate or Bunsen burner
5.      Funnel
6.      Drying oven
7.      Paper towel
  
PROCEDURE:

1.      Weigh the dry pycnometer to nearest 0.01 gram and record it as W1.
2.      Take about 100 grams of oven dried soil and put it into the flask. Weigh the flask and dry soil to the nearest 0.01 gram. Record this weight as W2.
3.      Add water in the pycnometer until it is about two-third full. In order to remove the entrapped air from soil and water, heat the mixture for at least 2 h after the soil-water mixture comes to a full boil. Use only enough heat to keep the slurry boiling. Agitate the slurry as necessary to prevent any soil from sticking to or drying onto the glass above the slurry surface.
4.      Allow the mixture to cool, and then fill the flask with distilled water to above the calibration mark.
5.      Place the stopper in the bottle while removing the excess water. Be sure the entire exterior of the flask is dry. Weigh the flask to the nearest 0.01 gram and record this weight as W3.
6.      Empty the flask, wash it thoroughly and fill it completely with water. Dry the exterior of the flask. Weigh the flask and record it as W4.
7.      Repeat the procedure three times.
8.      Record the temperature of soil water mixture.


PRECAUTIONS

1.      Make sure no air is entrapped within the soil water mixture.
2.      Weights should be obtained from a properly balanced weighing scale.

OBSERVATIONS AND CALCULATIONS

Test No.
1
2
3
Volume of flask



W1 (grams)



W2 (grams)



W3 (grams)



W4 (grams)



a



Gs




Typical values of correction factor, α;
T (oC)
Correction Factor, α
4
1.0000
15
0.9999
20
0.9982
25
0.9971
30
0.9957
35
0.9941

REFERENCE

ASTM D854 – 02
Standard Test Methods for Specific Gravity of Soil Solids by Water Pycnometer

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